Physico-chemical analysis

01Prerequisites

You need to analyze the material health of your raw materials for production monitoring, part and/or material validation, or R&D purposes.

Etim carries out a wide range of thermal and physico-chemical analyses on raw materials and composite materials, polymers and elastomers, in compliance with existing standards or to our customers’ own specifications…

If you want to compare products, check that your process has been properly transformed, obtain the characteristics needed to size a part or analyze pollution, we can help you analyze your needs and define the right test(s) to carry out.

Our qualifications for the aeronautic’s sector with our specific customer accreditations (AIRBUS, SAFRAN, DASSAULT, etc.) cover a wide spectrum of analyses.

Etim can meet your needs for series production follow-up testing within short deadlines ranging from 1 to 10 days maximum.

Our laboratory is operational all year round, with teams working 2*8 shifts.

02Technical resources

  • DMA (from -150 to 600 °C / single and double flush mounting, bending, torsion, …)
  • TMA (-150 to 1000 °C / expansion-penetration-traction probes)
  • TMA cryogenic (-269°C à +200°C / expansion-penetration-traction probes) – NEW
  • DSC (-80 to 550°C)
  • Modulated DSC (from -80 to 550°C)
  • ATG (from 23 to 1000°C)
  • Plastometer (from 50 to 450 °C – from 0.325 to 21.6 kg)
  • FTIR infrared microscope
  • µIRTF infrared microscope
  • Rheometer (-160 to 600 °C; DMA by torsion)
  • Means for TVF (Fiber Volumic Rate) by acid digestion (acid T°C from 160 to 260 °C)
  • Calcination furnaces (up to 1100°C)

03Our services

All our equipment guarantees results in line with current standards (ISO, EN, NF, ASTM, AITM, IGC, etc.).

Thermal analysis

  • ​ATG: mass loss of a material during degradation at temperature and in an oxidizing or inert atmosphere, residue rate of a composite material (glass fibers, carbon, etc.), etc.
  • DSC: determination of a material’s thermal transitions (glass transition, melting temperature/enthalpy, crystallization temperature/enthalpy, polymerization rate, crystallinity rate, etc.), specific heat, oxidation induction time, etc.
  • DMA: measurement of storage modulus, loss, glass transition, master curve (frequency and amplitude variation, etc.)
  • TMA: Measurement of a material’s coefficient of linear expansion from -150 to 1000°C (coefficient of thermal expansion, glass transition temperature, etc.) and for cryogenic condition with measurement from -269°C à +200°C

Physico-chemical analysis

  • Density measurement (pycnometer method)
  • TVF by acid digestion or dissolution: determination of fiber and resin mass ratios, determination of fiber, resin and porosity volume ratios
  • Surface mass measurement
  • Volatile content measurement
  • Measurement of ash content
  • Flow rate measurement
  • Measurement of water content
  • Measurement of gel time, polymerization kinetics
  • Density and melt flow index measurement
  • FTIR spectrometry analysis: determination of the chemical nature of polymers/paints/adhesives, identification of pollution, identification of organic or inorganic residues…​

04Standards and accreditations


Standards and accreditations

ESSAIS PHYSICO-CHIMIQUES (Chimical-Physical Testing) Spécification
NADCAP
AIRBUS
SAFRAN
DASSAULT
DMA AITM 1-0003
ASTM D7028
ASTM E1640
NF EN ISO 6721-1
ISO 6721-4
ISO 6721-5
ISO 6721-6
ISO 6721-10
ISO 6721-11
NF EN 6032
DSC AITM 3-0002
AITM 3-0008
AITM 3-0027
ASTM D3418
NF EN 6041
NF EN ISO 11357
DSC modulée (DSC modulated) ASTM E2602
ASTM E2716
Flux de résine (Resin Flow) NF EN 2560
IGC 04-26-225
Imprégnation (impregnation) AITM 2-0061
Masse surfacique (Fiber Mass per unit area) NF EN 2329
NF EN 2557
Masse Volumique/ densité (Density) NF EN ISO 1183
NF EN ISO 845
ASTM D792
Rhéologie - temps de gel, viscosité (Rheology - gel time, viscosity) EN 6043
Spectroscopie IR (Spectroscopie IRTF) NF ISO 4650
Taux de fibres (fiber rate) ASTM D3171
NF EN 2331
NF EN 2559
NF EN 2564
NF EN ISO 1172
NF EN ISO 3451-1
Porosité (Porosity) ASTM D2734
Taux de volatils (Volatil content) ASTM D3530
NF EN 2330
NF EN 2558
ATG (TGA) NF EN ISO 11358-1
NF T46-047
TMA ASTM E831
ISO 11359-1
ISO 11359-2
ISO 11359-3

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